도금량 측정 기기용 표준 시료 개발

목차

1. 서론

2. 연구 방법

2. 1. 형광 X 선에 의한 부착량 및 조성 측정 방법

2.2. 표준 시료 제조

2.3. 표준 시료의 도금 부착량과 조성 분석

3. 실험 결과

3.1. 표준 시료의 부착량 및 조성 편차

3.2. 표준 시료의 표면 특성

3.3. XRF에 의한 검량선 작성

4. 결론

5. 참고 문헌

본문내용

기대되며, 도금 제품의 품질 확보에 기여 할 수 있으리라 판단된다.
5. 참고 문헌
(1) R. Tertian and F. Claisse, Principles of quantitative X-ray fluorescence analysis, Heyden & Son Ltd, 1982.
(2) K. Tsumura and S. Oshiba, 鐵と鋼, Vol 7, 1170, 1977.
(3) 신광수, 홍기정, 박병학, 전기도금강판의 합금층 분석 연구, RIST 연구결과보고서, 1988.
(4) C. Whiston, X-ray methods, Joh, Wiley & Sons, pp268-279, 1987.
(5) D. Laguitton and W. Parrish, Anal. chem. Vol.49, No.8, 1152, 1977.
(6) J.F. Butler, J. vac. sci. & technol., Vol.7, No.1, S52.
(7) 이영호, 측정 표준 Vol. 17, No.4, 56, 1994.
Figure and photo caption
Fig. 1 X-ray flourescence from coating
Fig. 2 Auger depth profiles of Zn-Fe coated samples
Fig. 3 Zn XRF intensity as a function of coating weight
Fig. 4 Comparision of coating weight measured by chemical vs XRF method
Fig. 5 Comparision of coating weight measured by chemical vs XRF method
Fig. 6 Zn Kα and Zn Lα intensity as a function of coating weight
Fig. 7 Zn Lα intensity as a function of coating weight
Photo 1 Photograph of standard reference samples
Photo 2 Selected SEM image of Zn coated samples(coating weight increases as a to d)
Photo 3 Selected SEM image of Zn-Fe coated samples (coating weight increases as a to d)
X-ray Zn Lα Zn Kα
Fe Kα
θ
Zn(A) t
Fe(B)
Figure and photo caption
Fig. 1 X-ray flourescence from coating
Fig. 2 Auger depth profiles of Zn-Fe coated samples
Fig. 3 Zn XRF intensity as a function of coating weight
Fig. 4 Comparision of coating weight measured by chemical vs XRF method
Fig. 5 Comparision of coating weight measured by chemical vs XRF method
Fig. 6 Zn Kα and Zn Lα intensity as a function of coating weight
Fig. 7 Zn Lα intensity as a function of coating weight
Photo 1 Photograph of standard reference samples
Photo 2 Selected SEM image of Zn coated samples
Photo 3 Selected SEM image of Zn-Fe coated samples

키워드

도금량 측정,   기기용 표준 시료